You can't do that. Instead, you should create a class that contains these two properties, then you can create an array of that type:
public class MyClass
{
public string ControlName {get;set;}
public bool MyBooleanValue {get;set;}
}
public MyClass[] myValues=new MyClass[numberOfItems];
Or, as Anders says, use a dictionary if one of the properties is meant to be used to perform lookups.
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